Calibration

The description of the gas chromatograph calibration process can be found here.

Analysis

• Inject test sample of rakia at least three times.



• Process sample chromatograms.



• Using equation below, calculate the concentration of each congener in the samples.



• As a result of calculations, the values ​​of the concentrations of analytes in the dimension mg/L AA.

Compound	Calibration					Analysis
	Certificate, mg/L AA	Response 1, a.u.	Response 2, a.u.	Response 3, a.u.	RRF	Response, a.u.	Concentration, mg/L AA
Acetaldehyde	428.250	26.548	26.676	26.955	1.224	8.500	113.399
Methyl acetate	682.510	34.498	33.961	34.613	1.517	-	-
Ethyl acetate	616.510	43.492	42.927	43.733	1.085	78.853	932.933
Acetal	552.980	52.283	51.473	52.633	0.810	11.349	100.232
Methanol	481.410	31.720	31.521	31.966	1.159	410.676	5186.655
Ethanol	789300	60268	59835	60761	1.000	72412	789300
2-butanol	497.890	60.212	59.785	60.769	0.631	-	-
1-propanol	484.060	57.201	56.777	57.634	0.646	42.238	297.673
2-methyl-1-propanol	474.360	66.381	65.845	66.873	0.546	28.150	167.514
3-pentanol	536.020	71.437	70.809	71.924	0.573	70.883	443.107
1-butanol	496.770	64.686	64.272	65.238	0.586	8.647	55.246
2-methyl-1-butanol	514.010	72.918	72.392	73.344	0.539	10.901	64.008
3-methyl-1-butanol	492.710	69.622	69.173	70.083	0.541	60.996	359.372